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Author: Joseph D. Menczel
Publisher: John Wiley & Sons
ISBN: 1118995996
Category : Science
Languages : en
Pages : 696
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Book Description
Presents a solid introduction to thermal analysis, methods,instrumentation, calibration, and application along with thenecessary theoretical background. Useful to chemists, physicists, materials scientists, andengineers who are new to thermal analysis techniques, and toexisting users of thermal analysis who wish expand their experienceto new techniques and applications Topics covered include Differential Scanning Calorimetry andDifferential Thermal Analysis (DSC/DTA), Thermogravimetry,Thermomechanical Analysis and Dilatometry, Dynamic MechanicalAnalysis, Micro-Thermal Analysis, Hot Stage Microscopy, andInstrumentation. Written by experts in the various areas of thermalanalysis Relevant and detailed experiments and examples follow eachchapter.
Author: Joseph D. Menczel
Publisher: John Wiley & Sons
ISBN: 1118995996
Category : Science
Languages : en
Pages : 696
Get Book
Book Description
Presents a solid introduction to thermal analysis, methods,instrumentation, calibration, and application along with thenecessary theoretical background. Useful to chemists, physicists, materials scientists, andengineers who are new to thermal analysis techniques, and toexisting users of thermal analysis who wish expand their experienceto new techniques and applications Topics covered include Differential Scanning Calorimetry andDifferential Thermal Analysis (DSC/DTA), Thermogravimetry,Thermomechanical Analysis and Dilatometry, Dynamic MechanicalAnalysis, Micro-Thermal Analysis, Hot Stage Microscopy, andInstrumentation. Written by experts in the various areas of thermalanalysis Relevant and detailed experiments and examples follow eachchapter.
Author: W.M. Groenewoud
Publisher: Elsevier
ISBN: 9780080528939
Category : Technology & Engineering
Languages : en
Pages : 396
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Book Description
Thermal Analysis (TA) has become an indispensable family of analytical techniques in the polymer research. The increased importance of these techniques can be seen as the result of three more or less parallel developments: • a tempestuous development of TA measuring techniques in combination with a high degree of automation, • the strongly increased understanding of the underlaying theory and, • the increasing knowledge of the relation between the polymers' chemical structure and their physical properties. These areas are still in their developmental stages, especially the third area. The increasing knowledge of the dependence of physical properties on chemical structure just accentuated more and more the need for accurate thermoanalytical measurements, and this knowledge is very important for the first stages of the development of new polymeric systems. Besides, the contribution of TA remains necessary for the technical and commercial development of such a new polymer system. The use of the various TA techniques in these processes is described in this book in nine chapters, while chapter ten illustrates the information obtained about different polymers during special case studies. This book illustrates in this way, applications of a wide variety of TA techniques whilst it is written from a materials characterisation rather than from a TA point of view with attention being paid to the chemical structure/physical properties correlations.
Author: Edith Turi
Publisher: Elsevier
ISBN: 0323141889
Category : Technology & Engineering
Languages : en
Pages : 986
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Book Description
Thermal Characterization of Polymeric Materials is a critical review and a concise evaluation of the application of thermal analysis in polymer science and engineering. This book is divided into nine chapters that specifically tackle the instrumentation, theory, and a wide variety of applications of thermal characterization. The introductory chapters provide an overview of all aspects of thermal analytical methods and apparatus and the theory underlying the basic principles of thermal analysis. These chapters also examine the theories and functions of state for thermometry, dilatometry, thermomechanical analysis, calorimetry, thermogravimetry. These topics are followed by a discussion on single-component and multicomponent systems and their phase transitions, as influenced by concentration, pressure, deformation, molecular weight, and copolymerization. The subsequent chapters explore the influence of important chemical and physical parameters on the glass transition, crystallization, and melting of thermoplastic materials. The discussion then shifts to the theoretical aspects of polymer-polymer compatibility, phase separation, and miscibility in mixed polymer systems. This book further considers the thermal analysis in thermosets, elastomers, and fibers. The concluding chapters present the methods of obtaining information on the relative flammability properties of polymers, for screening fire retardant additives, and for studying the mechanism of flame inhibition. These chapters also look into the thermal analysis of antioxidants, stabilizers, lubricants, plasticizers, impact modifiers, and fire retardants. Polymer scientists and researchers will find this book invaluable.
Author: M. P. Sepe
Publisher: iSmithers Rapra Publishing
ISBN: 9781859571071
Category : Technology & Engineering
Languages : en
Pages : 130
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Book Description
The techniques which are particularly relevant to polymer characterisation are evaluated in this new report. For each technique the author describes the method of operation and the output obtained, and then considers its application to polymer characterisation. An additional indexed section containing several hundred abstracts from the Rapra Polymer Library database provides useful references for further reading.
Author: Wiley
Publisher: John Wiley & Sons
ISBN: 0470233001
Category : Technology & Engineering
Languages : en
Pages : 987
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Book Description
Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.
Author: Edith A. Turi
Publisher:
ISBN: 9780127037837
Category :
Languages : en
Pages :
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Book Description
Author: Dan Campbell
Publisher: CRC Press
ISBN: 1482268361
Category : Technology & Engineering
Languages : en
Pages : 492
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Book Description
Discerning the properties of polymers and polymer-based materials requires a good understanding of characterization. This revised and updated text provides a comprehensive survey of characterization methods within its simple, concise chapters. Polymer Characterization: Physical Techniques, provides an overview of a wide variety of characterization methods, which makes it an excellent textbook and reference. It starts with a description of basic polymer science, providing a solid foundation from which to understand the key physical characterization techniques. The authors explain physical principles without heavy theory and give special emphasis to the application of the techniques to polymers, with plenty of illustrations. Topics covered include molecular weight determination, molecular and structural characterization by spectroscopic techniques, morphology and structural characterization by microscopy and diffraction, and thermal analysis. This edition contains a new chapter on surface analysis as well as some revised problems and solutions. The concise treatment of each topic offers even those with little prior knowledge of the subject an accessible source to relevant, simple descriptions in a well-organized format.
Author: Mike Reading
Publisher: Springer Science & Business Media
ISBN: 1402037503
Category : Technology & Engineering
Languages : en
Pages : 340
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Book Description
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Author: Jen Chiu
Publisher:
ISBN:
Category : Detroit, MI
Languages : en
Pages : 272
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Book Description
Author: T.R Crompton
Publisher: Smithers Rapra
ISBN: 184735663X
Category : Science
Languages : en
Pages : 256
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Book Description
This book reviews the various thermal methods used for the characterisation of polymer properties and composition. All these methods study the properties of polymers as they change with temperature. The methods discussed in this book are: differential photocalorimetry, differential scanning calorimetry, dielectric thermal analysis, differential thermal analysis, dynamic mechanical analysis, evolved gas analysis, gas chromatography, gas chromatography combined with mass spectrometry, mass spectrometry, microthermal analysis, thermal volatilisation, thermogravimetric analysis and thermomechanical analysis. Each technique is discussed in detail and examples of the use of each technique are also given. Each chapter has an extensive list of references so that the reader can follow up topics of interest. This book will be a useful reference for those who already use any of these thermal methods but will also be of interest to undergraduates and those who are just starting to use these techniques.
